Custom manufacturing
Basic information
Nippon Chemical Industrial has supplied phosphorus compounds, organic and inorganic, for many years. Based on accumulated experience, we have technology available to offer customsynthesis service for semiconductor, pharmaceutical, and agricultural chemical industries, etc.
We provide solutions to meet your demands, including impurity control at an industrial scale level, analysis of minute impurities in the product, and exploration of optimal synthesis route involving combination of company ingredients and coupling ligands.
Pilot plant
We are flexible in manufacturing scale for early phase, from laboratory scale to pilot plant. For mass production, we have the facilities available for various scales. Please feel free to inquire us.
Main Reactors
Volume | Material | Type of agitator | Remark | |
---|---|---|---|---|
Main Rector#1 | 500L | GL | MAXBLEND® | - |
Main Rector#2 | 500L | GL | FULLZONE® | - |
Main Rector#3 | 500L | GL | 3pieces swept-back wing | Class-1 pressure vessel |
Main Rector#4 | 500L | Has/C | Two-tiered four paddle blades | - |
Filter and Dryer
Volume | Material | Type of agitator | Remark | |
---|---|---|---|---|
Centrifugal separator | 80L | Aflon® | - | - |
Conical dry blende | 550L | GL | - | - |
Filter dryer | 300L | GL | Special agitator | Filtration area 0.3m2 |
Distllation Equipment
Volume | Material | Type of agitator | Remark | |
---|---|---|---|---|
Evaporator | 100L | SUS316L | Inclined paddle blade | ~ 270℃ |
Anchor blade | ||||
Reciever#1 | 100L | SUS316L | - | - |
Reciever#2 | 50L | SUS316L | - | - |
Distillation columns | - | SUS316L | - | 5 theoretical plates |
Others
Vacuum pumps | Water-sealed pump, dry pump |
---|---|
Scrubber | FRP two-column type 60m3/min |
Refrigerator | 18.2 refrigerating ton * 2 units |
Extremely low temp. refrigerator | LN2 MAX-85℃ |
Water deionizer | 1 unit |
Available reaction
・Wittig Reaction
・Arbzov Reaction
・Halogenation
・Friedel Crafts Reaction
・Diazotization
・Asymmetric Hydrogenation
・Oxidation
Mukaiyama Oxidation
Hydrogen peroxide
Oxone
・Reduction
NaBH4
・Organic Phosphorus general reaction
Alkyl Phosphine
Please contact us for inquiries about Consigned synthesis.